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Specifics of hydrothermal synthesis of oriented zinc oxide nanorods on metallic zinc substratesстатья
Информация о цитировании статьи получена из
Web of Science,
Scopus
Статья опубликована в журнале из списка Web of Science и/или Scopus
Дата последнего поиска статьи во внешних источниках: 18 июля 2013 г.
- Авторы: Gavrilov A.I., Kapitanova O.O., Baranov A.N., Churagulov B.R.
- Журнал: Russian Journal of Inorganic Chemistry
- Том: 57
- Номер: 9
- Год издания: 2012
- Издательство: Maik Nauka/Interperiodica Publishing
- Местоположение издательства: Russian Federation
- Первая страница: 1182
- Последняя страница: 1186
- DOI: 10.1134/S0036023612090069
- Аннотация: Zinc oxide nanostructures are prepared hydrothermally in the presence of ethylenediamine (EDA). The morphology and photoluminescent properties of final products are studied as functions of synthesis temperature, synthesis time, and EDA concentration. A decrease in EDA concentration to 30% favors the formation of more perfect and more ordered structures. Blank experiments show that hydrothermal synthesis without organic reagents does not produce nanostructures. When samples are sheltered from convective flows in the cell, the rod growth direction is dictated by the grain orientation in the foil. When nanorods are formed under low supersaturations (in the absence of convective flows), oxygen nonstoichiometry arises in the nanorods and appears in photoluminescence spectra as increased peak intensities in the green spectral range.
- Добавил в систему: Баранов Андрей Николаевич